HRID1078762

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID27013

5,6,7,8-Tetrahydro[1,3]dioxolo[4,5-g]isoquinoline

C10H11NO2

HCID10812203

未命名化合物

PRODUCTS

生成物

结构：COc1ccc(C(CCCCCN2CCc3cc4c(cc3C2)OCO4)Sc2ccc(C)cc2)cc1OC

HCID10577864

未命名化合物

收率 91.7%

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID6342

Acetonitrile

C2H3N

PROCEDURE

实验过程

The procedure of Example 46 is repeated using 3.67 g of 4-[6-bromo-1-[(4-methylphenyl)thio]hexyl]-1,2-dimethoxybenzene in 40 mL of acetonitrile and 2.65 g of 6,7-methylenedioxy-1,2,3,4-tetrahydroisoquinoline. This affords 4.13 g of the desired product as a yellow gum.