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HRID1078798

反应详情

EQUATION

反应方程式

HRID 1078798 的结构方程式

REACTANTS

反应物

2
结构：O
HCID962

Water

H2O

结构：CC[O-].N[C@@H](C(=O)N[C@@H]1C(=O)N2C(C(=O)O)=C(Cl)CC[C@H]12)c1ccccc1
HCID86748663

未命名化合物

PRODUCTS

生成物

1
结构：N[C@@H](C(=O)NC1C(=O)N2C(C(=O)O)=C(Cl)CCC12)c1ccccc1.O
HCID60746

未命名化合物

PROCEDURE

实验过程

Loracarbef ethanolate, (4.0 g, 97.1% potency), was slurried in 56 ml of water (containing 0.004 eq sodium, ~0.02 g editate) at 50° C. for 2 hours. Within 30 minutes the slurry became very thick, indicating conversion to monohydrate. The product was vacuum filtered, washed with a minimum amount of water, and dried in a 40° C. vacuum oven. X-ray-confirmed as monohydrate.

WORKUP

后处理

  1. filtrationfiltered
  2. washwashed with a minimum amount of water
  3. customdried in a 40° C. vacuum oven