HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 54223889, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | HCID 53990882 | HCID 53990882 | — |
| Product | HCID 54223889 | HCID 54223889 | — |
Reaction Steps
A 282 mg portion of (4aR)-(10bR)-10b-methyl-8-(2-naphthylthio)-1,2,3,4,4a, 5,6,10b-octahydrobenzo [f]quinolin-3-one was methylated with methyl iodide following the process of Example 95 to obtain 137 mg of the desired product. mp 138°-139.5° FDMS: m/e=387. α[D]589 =+69.6, α[D]365 =+261.4 (chloroform).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05550134 |
| Source dataset | uspto-grants-1996_08 |
| ORD ID | ord-ae1bb600642b49278daf4175f189373d |
| Source note | uspto-grants-1996_08 |