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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1079270Generated: October 30, 2026

Chlorotitaniumtriisopropoxide → HCID 178459128, compound

https://huagongshe.com/reaction/1079270

Reaction equation

Participants

RoleNameHCIDCharge
ReactantChlorotitaniumtriisopropoxideHCID 11673339—
ReactantHCID 178425074HCID 178425074—
SolventDiethyl EtherHCID 3283—
ProductHCID 178459128HCID 178459128—

Reaction Conditions

Temperature-78 °C

Reaction Steps

A solution of 10 mmoles of 3,5-dimethylphenylmagnesium bromide in 10 mL of ether was cooled to -78° C. under nitrogen and to this was added 10 mL of a 1M solution of chlorotitanium triisopropoxide. The solution was stirred at -78° C. for 30 minutes and used in the next step.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05550233
Source datasetuspto-grants-1996_08
ORD IDord-2f8d3ae76c4446ef84c2f55de743bdec
Source noteuspto-grants-1996_08