関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | HCID 23366620 | HCID 23366620 | — |
| 溶媒 | Trifluoroacetic acid | HCID 6422 | — |
| 生成物 | N-Benzoylbenzylamine | HCID 73878 | — |
反応手順
N-benzoyl-2,4-dimethoxybenzylamine (100 mg, 0.37 mmol) was dissolved in 1 ml 95% (v/v) trifluoroacetic acid (TFA) and stirred for 1 h at 20° C. TFA was removed by blowing with N2 and the residue suspended in methanol (1 ml). The reaction mixture was analyzed by TLC using CH2Cl2 /MeOH/AcOH (85:10:5) as eluent and the generated benzamide was determined quantitatively by HPLC using benzamide standard chromatograms.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| 特許番号 | US05580751 |
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| 出典データセット | uspto-grants-1996_12 |
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| ORD ID | ord-559beeee2eff4a7388ab6c2ea27e7cde |
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| 出典メモ | uspto-grants-1996_12 |
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