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HRID 1079298作成日:2026年10月25日

HCID 23366620、化合物 → N-Benzoylbenzylamine

https://huagongshe.com/reaction/1079298

反応式

関与物質

役割名称HCID仕込み量
反応物HCID 23366620HCID 23366620—
溶媒Trifluoroacetic acidHCID 6422—
生成物N-BenzoylbenzylamineHCID 73878—

反応条件

温度20 °C

反応手順

N-benzoyl-2,4-dimethoxybenzylamine (100 mg, 0.37 mmol) was dissolved in 1 ml 95% (v/v) trifluoroacetic acid (TFA) and stirred for 1 h at 20° C. TFA was removed by blowing with N2 and the residue suspended in methanol (1 ml). The reaction mixture was analyzed by TLC using CH2Cl2 /MeOH/AcOH (85:10:5) as eluent and the generated benzamide was determined quantitatively by HPLC using benzamide standard chromatograms.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US05580751
出典データセットuspto-grants-1996_12
ORD IDord-559beeee2eff4a7388ab6c2ea27e7cde
出典メモuspto-grants-1996_12