HuagongsheHuagongshe Chemistry Print Report · For research reference only
Neopentyl glycol → 5,5-Dimethyl-2-(4-nitrobenzyl)-1,3,2-dioxaphosphorinan-2-oxide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Neopentyl glycol | HCID 31344 | — |
| Reactant | (4-Nitro-benzyl)-phosphonic acid | HCID 5180708 | — |
| Product | 5,5-Dimethyl-2-(4-nitrobenzyl)-1,3,2-dioxaphosphorinan-2-oxide | HCID 18928084 | — |
Reaction Steps
With 4-nitrobenzylphosphonic acid and 2,2-dimethyl-1,3-propanediol, the same procedure as in Reference Example 11 was followed, to yield 5,5-dimethyl-2-(4-nitrobenzyl)-1,3,2-dioxaphosphorinane-2-oxide, which was then recrystallized from ethanol-hexane to yield colorless plates having a melting point of 176° to 177° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05580863 |
| Source dataset | uspto-grants-1996_12 |
| ORD ID | ord-db131c60adf443c4bb56527500914b8e |
| Source note | uspto-grants-1996_12 |