Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
(3-Cyclopentyloxy-4-methoxyphenyl)(2-furyl)methanol → (3-Cyclopentyloxy-4-methoxyphenyl)-(2-furyl)ketone
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | (3-Cyclopentyloxy-4-methoxyphenyl)(2-furyl)methanol | HCID 19959391 | — |
| 촉매 | HCID 178418406 | HCID 178418406 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | (3-Cyclopentyloxy-4-methoxyphenyl)-(2-furyl)ketone | HCID 19959406 | 59.8% |
반응 단계
The alcohol (3.2 g) was stirred with manganese (IV) oxide (10 g) in CH2Cl2 (100 ml) at RT for 3 h. The mixture was filtered through Celite® and the filtrate concentrated in vacuo. The residual dark oil was subjected to chromatography (SiO2) to give (3-cyclopentyloxy-4-methoxyphenyl)-(2-furyl)ketone (1.9 g); νmax (neat) 1620 cm-1.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05580888 |
| 출처 데이터셋 | uspto-grants-1996_12 |
| ORD ID | ord-a284ae3d7018462ab5de879d577cc04f |
| 출처 메모 | uspto-grants-1996_12 |