Triethylamine → HCID 15839957, compound

Participants

Reaction Steps

1.5 ml of triethylamine and 0.7 ml of diethyl cyanophosphate were added to a suspension of 0.65 g of phenoxyacetic acid and 0.6 g of 2-nitroxyethylamine nitrate in 20 ml of tetrahydrofuran with ice-cooling. The mixture was stirred at room temperature for 2 hours and the solvent was distilled off under reduced pressure. The residue was purified by column chromatography through silica gel (eluent; hexane: ethyl acetate=1:1) and then recrystallized from diisopropyl ether to give 0.27 g of the title compound as colorless needles.

Provenance & Evidence