HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic acid, (3-methylphenoxy)- → N-(2-Nitroxyethyl)-3-methylphenoxyacetamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic acid, (3-methylphenoxy)- | HCID 74235 | — |
| Reactant | Ethanol, 2-amino-, 1-nitrate, nitrate (1:1) | HCID 78397 | — |
| Solvent | Hexane | HCID 8058 | — |
| Product | N-(2-Nitroxyethyl)-3-methylphenoxyacetamide | HCID 15839958 | 55.4% |
Reaction Steps
Following a similar treatment to that in Example 2 and using 0.71 g of 3-methylphenoxyacetic acid and 0.6 g of 2-nitroxyethylamine nitrate, 0.50 g of the title compound was obtained as colorless powdery crystals (solvent for recrystallization; hexane).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05580893 |
| Source dataset | uspto-grants-1996_12 |
| ORD ID | ord-393c2e144f7b4afcab952383460f260a |
| Source note | uspto-grants-1996_12 |