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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1079449Generated: October 25, 2026

Diisopropyl Ether → N-(2-Nitroxyethyl)-2-chlorophenoxyacetamide

https://huagongshe.com/reaction/1079449

Reaction equation

Participants

RoleNameHCIDCharge
ReactantDiisopropyl EtherHCID 7914—
Reactant2-Chlorophenoxyacetic acidHCID 11969—
ReactantEthanol, 2-amino-, 1-nitrate, nitrate (1:1)HCID 78397—
ProductN-(2-Nitroxyethyl)-2-chlorophenoxyacetamideHCID 1583995931.8%

Reaction Steps

Following a similar treatment to that in Example 2 and using 0.79 g of 2-chlorophenoxyacetic acid and 0.6 g of 2-nitroxyethylamine nitrate, 0.31 g of the title compound was obtained as colorless acicular prisms (solvent for recrystallization; diisopropyl ether).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05580893
Source datasetuspto-grants-1996_12
ORD IDord-86e39adc5cf340df89beffa4dbab0fd4
Source noteuspto-grants-1996_12