HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diisopropyl Ether → N-(2-Nitroxyethyl)phenylthioacetamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diisopropyl Ether | HCID 7914 | — |
| Reactant | Ethanol, 2-amino-, 1-nitrate, nitrate (1:1) | HCID 78397 | — |
| Reactant | HCID 178526157 | HCID 178526157 | — |
| Product | N-(2-Nitroxyethyl)phenylthioacetamide | HCID 86750043 | 66.9% |
Reaction Steps
Following a similar treatment to that in Example 2 and using 0.72 g of phenylthioacetic acid and 0.60 g of 2-nitroxyethylamine nitrate, 0.57 g of the title compound was obtained as colorless powdery crystals (solvent for recrystallization; diisopropyl ether).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05580893 |
| Source dataset | uspto-grants-1996_12 |
| ORD ID | ord-229cd61738d8413287cc82aeb51f2c4b |
| Source note | uspto-grants-1996_12 |