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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1079472Generated: October 25, 2026

Diisopropyl Ether → N-(2-Nitroxyethyl)-1,4-benzodioxane-2-carboxamide

https://huagongshe.com/reaction/1079472

Reaction equation

Participants

RoleNameHCIDCharge
ReactantDiisopropyl EtherHCID 7914—
ReactantEthanol, 2-amino-, 1-nitrate, nitrate (1:1)HCID 78397—
Reactant1,4-Benzodioxane-2-carboxylic acidHCID 2735450—
ProductN-(2-Nitroxyethyl)-1,4-benzodioxane-2-carboxamideHCID 6770835133.4%

Reaction Steps

Following a similar treatment to that in Example 2 and using 0.91 g of 1,4-benzodioxane-2-carboxylic acid and 0.85 g of nitroxyethylamine nitrate, 0.45 g of the title compound was obtained as colorless needles (solvent for recrystallization; diisopropyl ether).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05580893
Source datasetuspto-grants-1996_12
ORD IDord-79150892de004031b4d6a6f1d8523506
Source noteuspto-grants-1996_12