HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Furancarboxylic acid → HCID 23367113, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Furancarboxylic acid | HCID 6919 | — |
| Reactant | Diisopropyl Ether | HCID 7914 | — |
| Reactant | Ethanol, 2-amino-, 1-nitrate, nitrate (1:1) | HCID 78397 | — |
| Reactant | P,P-Diphenylphosphinic azide | HCID 199401 | — |
| Product | HCID 23367113 | HCID 23367113 | 59.1% |
Reaction Steps
Following a similar treatment to that in Example 2, using 0.34 g of 2-furancarboxylic acid and 0.50 g of nitroxyethylamine nitrate and using diphenylphosphoryl azide instead of ethyl cyanophosphate, 0.35 g of the title compound was obtained as colorless needles (solvent for recrystallization; diisopropyl ether).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05580893 |
| Source dataset | uspto-grants-1996_12 |
| ORD ID | ord-265a74691cc143bfb336d66dfe652028 |
| Source note | uspto-grants-1996_12 |