HRID1080375

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID12136

Benzyl carbamate

C8H9NO2

HCID15620607

Oxoacetic acid--water (1/1)

C2H4O4

PRODUCTS

生成物

HCID3509506

{[(Benzyloxy)carbonyl]amino}(hydroxy)acetic acid

C10H11NO5

收率 73%

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID3283

Diethyl Ether

C4H10O

PROCEDURE

实验过程

Benzyl carbamate (63 g, 0.05 mol) was stirred with glyoxylic acid monohydrate (5.09 g, 0.055 mol) in dry ether (50 mL). The crystalline product 22A (7.81 g, 73%) formed was filtered and washed with ether.