HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,7-dioxaspiro[4.4]nonane-1,6-dione → Carbon Dioxide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,7-dioxaspiro[4.4]nonane-1,6-dione | HCID 230907 | — |
| Solvent | Water | HCID 962 | — |
| Product | Carbon Dioxide | HCID 280 | — |
| Product | Oxane-4-carboxylic acid | HCID 219302 | — |
Reaction Steps
The 2,7-dioxaspiro[4.4]nonane-1,6-dione II can preferably be reacted in molten (m.p.: 108° to 109° C.) or dissolved form, together with the alcohol III or water and, if appropriate, an inert gas such as nitrogen, carbon dioxide or argon, to give tetrahydropyran-4-carboxylic acid and its esters I.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05580994 |
| Source dataset | uspto-grants-1996_12 |
| ORD ID | ord-41cf9cc62f5449d29ff108d95961b3db |
| Source note | uspto-grants-1996_12 |