HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,3-Dibromo-5,5-dimethylhydantoin → HCID 12717581, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,3-Dibromo-5,5-dimethylhydantoin | HCID 6479 | — |
| Reactant | Azobisisobutyronitrile | HCID 6547 | — |
| Reactant | Methyl p-tert-butylphenylacetate | HCID 605629 | — |
| Solvent | Carbon Tetrachloride | HCID 5943 | — |
| Product | HCID 12717581 | HCID 12717581 | — |
Reaction Steps
A solution of methyl 4-tert-butylphenylacetate (3.0 g), 1,3-dibromo-5,5-dimethylhydantoin (3.28 g) and azobisisobutyronitrile (AIBN, 0.01 g) in carbon tetrachloride (100 ml) was stirred in a 70° oil bath for hours. After cooling the mixture was filtered through Celite® and the filtrate was evaporated to give an oily residue of methyl α-bromo-4-tert-butylphenylacetate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05583147 |
| Source dataset | uspto-grants-1996_12 |
| ORD ID | ord-f774180a3ff74276a570e294afc82da6 |
| Source note | uspto-grants-1996_12 |