2-Propylvaleryl chloride → HCID 23363620, compound

HRID 1081251Notes

Reaction equation

HRID 1081251 reaction equation
[C:1](Cl)(=[O:9])[CH:2]([CH2:6][CH2:7][CH3:8])[CH2:3][CH2:4][CH3:5].Cl.[CH3:12][O:13][C:14](=[O:17])[CH2:15][NH2:16]>>[CH3:12][O:13][C:14](=[O:17])[CH2:15][NH:16][C:1](=[O:9])[CH:2]([CH2:6][CH2:7][CH3:8])[CH2:3][CH2:4][CH3:5]

Participants

3

Reactant 2

HCID 762402-Propylvaleryl chlorideHCID 122755Glycine methyl ester hydrochloride

Product 1

HCID 23363620HCID 23363620, compound

Procedure

The title compound was prepared from valproyl chloride (19.34 g, 119 mmole) and glycine methyl ester hydrochloride (15.0 g, 119 mmole), according to the procedure described in Ex. 4.22 g (102 mmole, 86%) of an off-white solid, mp 68° C., was thus obtained.

Sources & evidence

ORD record
ord-9ce9dbe9fdeb4a07b070a6e615a8a7f2
Source dataset
uspto-grants-1996_12
Patent number
US05585358

Reaction notes

Loading…