Methanol → HCID 10058100, compound

HRID 1081285Notes

Reaction equation

HRID 1081285 reaction equation
C(OC([N:11]([C:20]1[CH:25]=[C:24]([CH3:26])[CH:23]=[C:22]([CH3:27])[N:21]=1)[CH2:12][C:13]([NH:15]CC(N)=O)=O)=O)C1C=CC=CC=1.C[OH:29]>[Pd]>[CH3:26][C:24]1[CH:23]=[C:22]([CH3:27])[N:21]=[C:20]([NH:11][C:12](=[O:29])[CH2:13][NH2:15])[CH:25]=1

Participants

4

Reactant 2

HCID 887MethanolHCID 86749116HCID 86749116, compound

Product 1

HCID 10058100HCID 10058100, compound

Reagents, catalysts & solvents 1

HCID 23938PalladiumCatalyst

Procedure

1 g (2.6 mmol) of the product of Example 24 is dissolved in 60 ml of methanol. Palladium-on-carbon is added and the whole is stirred under a hydrogen atmosphere. Filtration is then carried out, the methanol is evaporated and the title product is recovered.

Workup

  1. filtrationFiltration
  2. customthe methanol is evaporated
  3. customthe title product is recovered

Sources & evidence

ORD record
ord-d8a9cff0e9f14288bb8a4c9310a127f1
Source dataset
uspto-grants-1996_12
Patent number
US05585390

Reaction notes

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