HuagongsheHuagongshe Chemistry Print Report · For research reference only
Toluene → 2-Pyridinecarboxylic acid, 3-(4-methylbenzoyl)-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Toluene | HCID 1140 | — |
| Reactant | Furo[3,4-b]pyridine-5,7-dione | HCID 69688 | — |
| Reactant | Aluminum(III) Chloride | HCID 6451240 | — |
| Product | 2-Pyridinecarboxylic acid, 3-(4-methylbenzoyl)- | HCID 10331901 | — |
Reaction Steps
Employing 2,3-pyridinedicarboxylic anhydride (10.0 g), toluene (125 ml) and aluminum chloride (15.0 g), substantially the same reaction and process as in Reference Example 1 Process 1 and Step 1 were conducted to give 3-(4-methylbenzoyl)-2-pyridinecarboxylic acid as colorless crystals (7.8 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05585385 |
| Source dataset | uspto-grants-1996_12 |
| ORD ID | ord-01b05a84a945428eadab4745bb0a0215 |
| Source note | uspto-grants-1996_12 |