HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Chloroaniline → HCID 12930160, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Chloroaniline | HCID 7932 | — |
| Reactant | 2,4-Dichloronitrobenzene | HCID 11899 | — |
| Reactant | Sodium Acetate | HCID 517045 | — |
| Solvent | Ethylene Glycol | HCID 174 | — |
| Product | HCID 12930160 | HCID 12930160 | — |
Reaction Steps
A mixture of 50 g of 2,4-dichloro-1-nitrobenzene, 40 ml of 3-chloroaniline and 43 g of anhydrous sodium acetate in 220 ml of ethylene glycol is refluxed for 72 hours. After cooling, the precipitate formed is filtered off and washed with water to give 39 g of the expected product after crystallization from iso ether. M.p.=112° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05585394 |
| Source dataset | uspto-grants-1996_12 |
| ORD ID | ord-b3634ae113834a4f959fe5342b97003f |
| Source note | uspto-grants-1996_12 |