4-Chloro-1,2-dinitrobenzene → HCID 22922588, compound

Participants

Reaction Steps

26 g of 2-aminoindane hydrochloride and then 20 g of 4-chloro-1,2-dinitrobenzene are added to a solution of sodium ethylate, prepared from 0.61 g of sodium and 200 ml of EtOH, and the mixture is stirred for 48 hours at RT. The solvent is evaporated off under vacuum, the residue is extracted with AcOEt, washed with water and dried over Na2SO4 and the solvent is evaporated off under vacuum to give 10.3 g of the expected product after crystallization from EtOH. M.p.=108° C.

Provenance & Evidence