HCID 23363035, compound → HCID 23363019, compound

HRID 1081680Notes

Reaction equation

HRID 1081680 reaction equation
[SH:1][C:2]1[NH:6][C:5]2[CH:7]=[CH:8][CH:9]=[CH:10][C:4]=2[N:3]=1.Cl.Cl[CH2:13][C:14]1[C:19]([CH3:20])=[C:18]([S:21][CH2:22][CH2:23][CH2:24][N:25]2[CH:29]=[CH:28][N:27]=[CH:26]2)[CH:17]=[CH:16][N:15]=1>>[N:25]1([CH2:24][CH2:23][CH2:22][S:21][C:18]2[CH:17]=[CH:16][N:15]=[C:14]([CH2:13][S:1][C:2]3[NH:6][C:5]4[CH:7]=[CH:8][CH:9]=[CH:10][C:4]=4[N:3]=3)[C:19]=2[CH3:20])[CH:29]=[CH:28][N:27]=[CH:26]1

Participants

3

Reactant 2

HCID 23363035HCID 23363035, compoundHCID 178527775HCID 178527775, compound

Product 1

HCID 23363019HCID 23363019, compound

Procedure

Following the procedure described in Example 1, the reaction of 2-mercapto-1H-benzimidazole with 2-chloromethyl-4-[3-(imidazol-1-yl)propylthio]-3-methylpyridine hydrochloride gives the title compound as a colorless solid after crystallization from diisopropyl ether; m.p. 145°-146° C.

Sources & evidence

ORD record
ord-bff9fc0861974389b6a193ce023c8616
Source dataset
uspto-grants-1996_12
Patent number
US05587389

Reaction notes

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