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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 1081777Erstellt: 25. Oktober 2026

5,6-Diamino-1,3-dimethyluracil → 1H-Purine-2,6-dione, 3,7-dihydro-1,3-dimethyl-8-(2-(2,5-dimethyl-4-methoxyphenyl)ethenyl)-, (E)-

https://huagongshe.com/reaction/1081777

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
Edukt5,6-Diamino-1,3-dimethyluracilHCID 79501—
Edukt4-Methoxy-2,5-dimethylcinnamic acidHCID 5199898—
Produkt1H-Purine-2,6-dione, 3,7-dihydro-1,3-dimethyl-8-(2-(2,5-dimethyl-4-methoxyphenyl)ethenyl)-, (E)-HCID 644897720%

Reaktionsschritte

Substantially the same procedure as in Example 7 was repeated using 1.0 g (5.88 mmol) of 5,6-diamino-1,3-dimethyluracil and 1.33 g (6.45 mmol) of 4-methoxy-2,5-dimethylcinnamic acid. Then, the resultant crude crystals were recrystallized from dimethylformamide to give 393 mg (yield 20%) of Compound 92 as pale yellow grains.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS05587378
Quelldatensatzuspto-grants-1996_12
ORD IDord-c0b1670ec08f490b8fa2509b3fcfb3a6
Quellennotizuspto-grants-1996_12