HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 3126210, compound → 1H-Purine-2,6-dione, 3,7-dihydro-8-(2-(4-butoxyphenyl)ethenyl)-1,3-diethyl-, (E)-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 3126210 | HCID 3126210 | — |
| Reactant | 5,6-Diamino-1,3-diethyluracil | HCID 4572133 | — |
| Product | 1H-Purine-2,6-dione, 3,7-dihydro-8-(2-(4-butoxyphenyl)ethenyl)-1,3-diethyl-, (E)- | HCID 6448880 | 53% |
Reaction Steps
Substantially the same procedure as in Example 7 was repeated using 3.00 g (15.1 mmol) of 5,6-diamino-1,3-diethyluracil and 3.67 g (16.7 mmol) of 4-butoxycinnamic acid. Then, the resultant crude crystals were recrystallized from dioxane/water to give 3.04 g (yield 53%) of Compound 104 as pale yellow needles.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05587378 |
| Source dataset | uspto-grants-1996_12 |
| ORD ID | ord-99356b84e95c4a00a9a06ca133ffd16d |
| Source note | uspto-grants-1996_12 |