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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 1081784생성일: 2026년 10월 25일

3-(p-Tolyl)acrylic acid → 1H-Purine-2,6-dione, 3,7-dihydro-1,3-diethyl-8-(2-(4-methylphenyl)ethenyl)-, (E)-

https://huagongshe.com/reaction/1081784

반응식

참여 물질

역할이름HCID투입량
반응물3-(p-Tolyl)acrylic acidHCID 15835—
반응물5,6-Diamino-1,3-diethyluracilHCID 4572133—
생성물1H-Purine-2,6-dione, 3,7-dihydro-1,3-diethyl-8-(2-(4-methylphenyl)ethenyl)-, (E)-HCID 644888254%

반응 단계

Substantially the same procedure as in Example 7 was repeated using 3.00 g (15.1 mmol) of 5,6-diamino-1,3-diethyluracil and 2.70 g (16.7 mmol) of 4-methylcinnamic acid. Then, the resultant crude crystals were recrystallized from dioxane to give 2.64 g (yield 54%) of Compound 106 as pale yellow needles.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US05587378
출처 데이터셋uspto-grants-1996_12
ORD IDord-c1b5e647c6cc4cd993f635d7d69a708f
출처 메모uspto-grants-1996_12