Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
3-(p-Tolyl)acrylic acid → 1H-Purine-2,6-dione, 3,7-dihydro-1,3-diethyl-8-(2-(4-methylphenyl)ethenyl)-, (E)-
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 3-(p-Tolyl)acrylic acid | HCID 15835 | — |
| 반응물 | 5,6-Diamino-1,3-diethyluracil | HCID 4572133 | — |
| 생성물 | 1H-Purine-2,6-dione, 3,7-dihydro-1,3-diethyl-8-(2-(4-methylphenyl)ethenyl)-, (E)- | HCID 6448882 | 54% |
반응 단계
Substantially the same procedure as in Example 7 was repeated using 3.00 g (15.1 mmol) of 5,6-diamino-1,3-diethyluracil and 2.70 g (16.7 mmol) of 4-methylcinnamic acid. Then, the resultant crude crystals were recrystallized from dioxane to give 2.64 g (yield 54%) of Compound 106 as pale yellow needles.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05587378 |
| 출처 데이터셋 | uspto-grants-1996_12 |
| ORD ID | ord-c1b5e647c6cc4cd993f635d7d69a708f |
| 출처 메모 | uspto-grants-1996_12 |