HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Methoxy-3-methylcinnamic acid → 155271-40-2
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Methoxy-3-methylcinnamic acid | HCID 4213986 | — |
| Reactant | 5,6-Diamino-1,3-diethyluracil | HCID 4572133 | — |
| Product | 155271-40-2 | HCID 6448886 | 38.1% |
Reaction Steps
Substantially the same procedure as in Example 7 was repeated using 2.50 g (12.6 mmol) of 5,6-diamino-1,3-diethyluracil and 3.00 g (13.9 mmol) of 4-methoxy-3-methylcinnamic acid. Then, the resultant crude crystals were recrystallized from dimethylsulfoxide/water to give 1.70 g (yield 36%) of Compound 110 as white flocculent precipitates.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05587378 |
| Source dataset | uspto-grants-1996_12 |
| ORD ID | ord-81ba4121fb0443e4a66ab0258ae9dee0 |
| Source note | uspto-grants-1996_12 |