HuagongsheHuagongshe Chemistry Print Report · For research reference only
trans-2,4,5-Trimethoxycinnamic acid → 147700-53-6
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | trans-2,4,5-Trimethoxycinnamic acid | HCID 91131 | — |
| Reactant | 5,6-Diamino-1,3-dipropyl-2,4(1H,3H)-pyrimidinedione | HCID 5098605 | — |
| Product | 147700-53-6 | HCID 6448759 | 23% |
Reaction Steps
Substantially the same procedure as in Reference Example 1 was repeated using 2.00 g (8.85 mmol) of 5,6-diamino-1,3-dipropyluracil and 2.32 g (9.73 mmol) of 2,4,5-trimethoxycinnamic acid. Then, the resultant crude crystals were recrystallized from 2-propanol/water to give 870 mg (yield 23%) of Compound 22 as a pale yellow powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05587378 |
| Source dataset | uspto-grants-1996_12 |
| ORD ID | ord-346ac8a5b12e4d788042410419eff046 |
| Source note | uspto-grants-1996_12 |