HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methyl-3-phenylprop-2-enoic acid → 155271-64-0
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methyl-3-phenylprop-2-enoic acid | HCID 14541 | — |
| Reactant | 5,6-Diamino-1,3-diethyluracil | HCID 4572133 | — |
| Product | 155271-64-0 | HCID 6448910 | 50% |
Reaction Steps
Substantially the same procedure as in Example 7 was repeated using 2.00 g (10.1 mmol) of 5,6-diamino-1,3-diethyluracil and 1.80 g (11.1 mmol) of α-methylcinnamic acid. Then, the resultant crude crystals were recrystallized from ethanol/water to give 1.63 g (yield 50%) of Compound 134 as white needles.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05587378 |
| Source dataset | uspto-grants-1996_12 |
| ORD ID | ord-070e1c63bb64424b9004ce04ca61ff4e |
| Source note | uspto-grants-1996_12 |