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HRID 1081855作成日:2026年10月25日

3',4'-Dimethoxycinnamic acid → 1H-Purine-2,6-dione, 3,7-dihydro-8-(2-(3,4-dimethoxyphenyl)ethenyl)-1,3-di-2-propenyl-, (E)-

https://huagongshe.com/reaction/1081855

反応式

関与物質

役割名称HCID仕込み量
反応物3',4'-Dimethoxycinnamic acidHCID 16848—
反応物1,3-Diallyl-5,6-diaminouracilHCID 13525062—
生成物1H-Purine-2,6-dione, 3,7-dihydro-8-(2-(3,4-dimethoxyphenyl)ethenyl)-1,3-di-2-propenyl-, (E)-HCID 644897254.2%

反応手順

Substantially the same procedure as in Reference Example 1 was repeated using 2.9 g (13.1 mmol) of 1,3-diallyl-5,6-diaminouracil and 2.99 g (14.4 mmol) of 3,4-dimethoxycinnamic acid. Then, the resultant crude crystals were recrystallized from dioxane/water to give 2.80 g (yield 54%) of Compound 190 as pale yellow flocculent precipitates.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US05587378
出典データセットuspto-grants-1996_12
ORD IDord-414349ad2ed3460e8ca1e0bede9427d4
出典メモuspto-grants-1996_12