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3',4'-Dimethoxycinnamic acid → 1H-Purine-2,6-dione, 3,7-dihydro-8-(2-(3,4-dimethoxyphenyl)ethenyl)-1,3-di-2-propenyl-, (E)-
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 3',4'-Dimethoxycinnamic acid | HCID 16848 | — |
| 反応物 | 1,3-Diallyl-5,6-diaminouracil | HCID 13525062 | — |
| 生成物 | 1H-Purine-2,6-dione, 3,7-dihydro-8-(2-(3,4-dimethoxyphenyl)ethenyl)-1,3-di-2-propenyl-, (E)- | HCID 6448972 | 54.2% |
反応手順
Substantially the same procedure as in Reference Example 1 was repeated using 2.9 g (13.1 mmol) of 1,3-diallyl-5,6-diaminouracil and 2.99 g (14.4 mmol) of 3,4-dimethoxycinnamic acid. Then, the resultant crude crystals were recrystallized from dioxane/water to give 2.80 g (yield 54%) of Compound 190 as pale yellow flocculent precipitates.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05587378 |
| 出典データセット | uspto-grants-1996_12 |
| ORD ID | ord-414349ad2ed3460e8ca1e0bede9427d4 |
| 出典メモ | uspto-grants-1996_12 |