HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydroxylamine → HCID 15389456, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydroxylamine | HCID 787 | — |
| Reactant | 3-(Dibenzylamino)butan-2-one | HCID 12440210 | — |
| Reactant | tert-Butyl 2-bromobutanoate | HCID 13124118 | — |
| Reactant | HCID 15389457 | HCID 15389457 | — |
| Product | HCID 15389456 | HCID 15389456 | — |
Reaction Steps
Examples 10 and 11 provide a detailed description for the preparation of (5S)-5-(N,N-dibenzylamino)-2-ethyl-4-oxo-hexanoic acid-tert-butyl ester from tert-butyl-2-bromobutyrate and α-(N,N-dibenzylamino)ethyl methyl ketone. This compound is reduced to the corresponding amino alcohol as described in detail above.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05587514 |
| Source dataset | uspto-grants-1996_12 |
| ORD ID | ord-213729b141184971b1ce39abacdb58dc |
| Source note | uspto-grants-1996_12 |