Ethanol, 2-amino-, 1-nitrate, nitrate (1:1) → HCID 69041746, compound

HRID 1082094Notes

Reaction equation

HRID 1082094 reaction equation
[C:1]([O:4][C:5]1[CH:13]=[CH:12][C:8]([C:9](Cl)=[O:10])=[CH:7][CH:6]=1)(=[O:3])[CH3:2].[N+]([O-])(O)=O.[N+:18]([O:21][CH2:22][CH2:23][NH2:24])([O-:20])=[O:19]>>[C:1]([O:4][C:5]1[CH:13]=[CH:12][C:8]([C:9]([NH:24][CH2:23][CH2:22][O:21][N+:18]([O-:20])=[O:19])=[O:10])=[CH:7][CH:6]=1)(=[O:3])[CH3:2]

Participants

3

Reactant 2

HCID 78397Ethanol, 2-amino-, 1-nitrate, nitrate (1:1)HCID 2756254p-Acetoxybenzoyl chloride

Product 1

HCID 69041746HCID 69041746, compoundYield 74.6%

Procedure

Starting from 0.113 mole of 4-acetoxybenzoic acid chloride and 0.110 mole of 2-nitrooxy-ethylamine nitrate, and operating substantially as described in the preceding Example, 22 g of the title compound were obtained. M.p. 95°-97° C. (ethyl ether).

Sources & evidence

ORD record
ord-1d328dc61ee8448aa2030c390b0f980f
Source dataset
uspto-grants-1996_12
Patent number
US05589490

Reaction notes

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