HCID 9956010, compound → HCID 23362235, compound

HRID 1082117Notes

Reaction equation

HRID 1082117 reaction equation
[O:1]1[C:5]2[CH:6]=[CH:7][CH:8]=[CH:9][C:4]=2[N:3]=[C:2]1[N:10]([CH2:12][CH2:13][O:14][C:15]1[CH:20]=[CH:19][C:18]([CH2:21][CH:22]([S:27][C:28]2[CH:33]=[CH:32][CH:31]=[CH:30][CH:29]=2)[C:23]([O:25]C)=[O:24])=[CH:17][CH:16]=1)[CH3:11]>ClCCl.CCCCCC>[O:1]1[C:5]2[CH:6]=[CH:7][CH:8]=[CH:9][C:4]=2[N:3]=[C:2]1[N:10]([CH2:12][CH2:13][O:14][C:15]1[CH:20]=[CH:19][C:18]([CH2:21][CH:22]([S:27][C:28]2[CH:33]=[CH:32][CH:31]=[CH:30][CH:29]=2)[C:23]([OH:25])=[O:24])=[CH:17][CH:16]=1)[CH3:11]

Participants

3

Reactant 1

HCID 9956010HCID 9956010, compound

Product 1

HCID 23362235HCID 23362235, compound

Reagents, catalysts & solvents 1

HCID 21226440Methylenechloride HexaneSolvent

Procedure

The title compound, mp 144°-7° C. (dichloromethane-hexane), was prepared from methyl 3-[4-[2-[N-(2-benzoxazolyl)-N-methylamino]ethoxy]phenyl]-2-(phenylthio)propanoate by a procedure similar to that described for Example 21.

Sources & evidence

ORD record
ord-c40dfc945c354822913056075fe4779f
Source dataset
uspto-grants-1996_12
Patent number
US05589492

Reaction notes

Loading…