HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonium fluoride → HCID 44284638, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonium fluoride | HCID 25516 | — |
| Reactant | HCID 67712795 | HCID 67712795 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 44284638 | HCID 44284638 | — |
Reaction Steps
(R)-15-(tert-Butyl-dimethylsilanyloxy)-13-methoxy-12-methyl-6,11-dioxo-3,4,5,6,7,8,9,11-octahydro-1H-10,2,5-benzoxathiaazacyclotridecine-4-carboxylic acid methyl ester was treated with ammonium fluoride in methanol in an analogous manner to the procedure described in Example 1 to yield (R)-15-hydroxy-13-methoxy-12-methyl-6,11-dioxo-3,4,5,6,7,8,9,11 -octahydro-1 H-10,2,5-benzoxathiaazacyclotridecine-4-carboxylic acid methyl ester as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05589473 |
| Source dataset | uspto-grants-1996_12 |
| ORD ID | ord-b2896850254d4d378d5a666765d1bbac |
| Source note | uspto-grants-1996_12 |