HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyrrolidine → Allyl 3-tetrahydropyrrolyl-2-butenoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyrrolidine | HCID 31268 | — |
| Reactant | Allyl acetoacetate | HCID 70701 | — |
| Product | Allyl 3-tetrahydropyrrolyl-2-butenoate | HCID 69629910 | — |
Reaction Steps
Allyl 3-tetrahydropyrrolyl-2-butenoate was prepared (4.7 g, 68%) in the same manner as described in the above Example 1 (1) from allyl acetoacetate (5.0 g, 35.17 mmol) and pyrrolidine (8.8 mL, 105.51 mmol), and the obtained product was identified with the following 1H NMR data.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07094908B2 |
| Source dataset | uspto-grants-2006_08 |
| ORD ID | ord-b23c8ba54c484e1bafaf208e0e2e4633 |
| Source note | uspto-grants-2006_08 |