1,6-Hexanediol → 6-Hydroxyhexyl Methacrylate (stabilized with MEHQ)
Reaction equation
OCCCC[CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][O:12][C:13](=[O:17])[C:14]([CH3:16])=[CH2:15].C(O)CCCCC[OH:24]>>[OH:24][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][O:12][C:13](=[O:17])[C:14]([CH3:16])=[CH2:15]Participants
3
Procedure
6-Hydroxyhexylmethacrylate was prepared using the same method as in the preparation of 10-hydroxydecylmethacrylate. 1,6-hexanediol was used instead of 1,10-decanediol. The same molar quantities of reactants were used. 11.5 g of product (62% yield) were collected.
Sources & evidence
- ORD record
- ord-ef4f6ec8873c47f6b52442067222ea4e
- Source dataset
- uspto-grants-1991_04
- Patent number
- US05004646
Reaction notes
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