HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoic Acid → Benzoic acid dicyclohexylamine salt
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoic Acid | HCID 243 | — |
| Reactant | Dicyclohexylamine | HCID 7582 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | Benzoic acid dicyclohexylamine salt | HCID 168040 | 90% |
Reaction Steps
Similarly, to a solution of 12.2 g (0.1 mol) of benzoic acid dissolved in 100 ml of acetone, 17.7 g (0.1 mol) of dicyclohexylamine was added dropwise. The crystals precipitated were filtered and then dried, and Benzoic acid dicyclohexylamine salt (molar ratio 1:1) of white crystals was obtained in an amount of 26.2 g (yield 90.0%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05004787 |
| Source dataset | uspto-grants-1991_04 |
| ORD ID | ord-e6a5e2fc0e694be782d4b9cf99fae02f |
| Source note | uspto-grants-1991_04 |