HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 20063239, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 21246577 | HCID 21246577 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 20063239 | HCID 20063239 | — |
Reaction Steps
The procedure of Example 2 was carried out in which (1-[(3-[(2,3-dihydro-2-oxo-5-phenyl-1,4-benzodiazepin-3-yl)methyl]-2,3-dihydro-1H-indol-1-yl) carbonyl]-3-methylbutyl]-carbamic acid-1,1-dimethylethyl ester was reacted with excess HCl gas in ethyl acetate at 0° C. to give the title compound as a foam.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05004741 |
| Source dataset | uspto-grants-1991_04 |
| ORD ID | ord-4f1c882c239a4df9a2ee4a544aeb5a28 |
| Source note | uspto-grants-1991_04 |