HuagongsheHuagongshe Chemistry Print Report · For research reference only
(4-Nitrophenyl)acetic acid → Ethanol, 2-[methyl[4-[2-(4-nitrophenyl)ethenyl]phenyl]amino]-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (4-Nitrophenyl)acetic acid | HCID 4661 | — |
| Reactant | Piperidine | HCID 8082 | — |
| Reactant | 4-[(2-Hydroxyethyl)(methyl)amino]benzaldehyde | HCID 3614316 | — |
| Product | Ethanol, 2-[methyl[4-[2-(4-nitrophenyl)ethenyl]phenyl]amino]- | HCID 180088 | — |
Reaction Steps
A one liter three-necked flask fitted with a dropping funnel, mechanical stirrer and condenser is charged with 34.35 g of 4-nitrophenylacetic acid, and piperidine (16.2 g) is added dropwise over a period of 30 minutes. At the end of the addition, a 33.62 g quantIty of 4-[N-(2-hydroxyethyl)-N-methylamino] benzaldehyde is added.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05006285 |
| Source dataset | uspto-grants-1991_04 |
| ORD ID | ord-564786c046584ae48598e88eddf98a22 |
| Source note | uspto-grants-1991_04 |