HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1084748Generated: November 1, 2026
Azobisisobutyronitrile → HCID 20062707, compound
https://huagongshe.com/reaction/1084748
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Azobisisobutyronitrile | HCID 6547 | — |
| Reactant | N-bromobutanimide | HCID 67184 | — |
| Reactant | HCID 20062669 | HCID 20062669 | — |
| Solvent | Carbon Tetrachloride | HCID 5943 | — |
| Product | HCID 20062707 | HCID 20062707 | — |
Reaction Steps
11 g of 3-(1-acetoxy-pentyl)toluene are dissolved in 100 ml of absolute carbon tetrachloride. After addition of 8.9 g of N-bromosuccinimide and 200 mg of azobisisobutyronitrile, the mixture is warmed slowly to the reflux temperature. When the reaction has ended, the mixture is heated under reflux for a further hour and then cooled to 0° C. and the succinimide is filtered off.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US05006534 |
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| Source dataset | uspto-grants-1991_04 |
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| ORD ID | ord-66189017478f46f491a8d7109a0f57d4 |
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| Source note | uspto-grants-1991_04 |
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