HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → Dimethyl 3-(1-naphthyl)-2-isoxazolin-5-ylphosphonate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Chlorosuccinimide | HCID 31398 | — |
| Reactant | Dimethyl vinylphosphonate | HCID 78376 | — |
| Reactant | 1-Naphthalenecarboxaldehyde, oxime | HCID 240801 | — |
| Product | Dimethyl 3-(1-naphthyl)-2-isoxazolin-5-ylphosphonate | HCID 20062404 | — |
Reaction Steps
Preparation is carried out in analogy to Example 1 from 31.2 g (0.2 mol) of 1-naphthaldoxime, 29.4 g (0.22 mol) of N-chlorosuccinimide, 29.2 ml (0.22 mol) of dimethyl vinylphosphonate and 30.6 ml (0.22 mol) of triethylamine, with 56 g of oily compound being obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05006515 |
| Source dataset | uspto-grants-1991_04 |
| ORD ID | ord-c8375bb701b14142941725e3d7153d4e |
| Source note | uspto-grants-1991_04 |