HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → Methyl 3-(1-naphthyl)-2-isoxazolin-5-yl(P-methyl)phosphinate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Chlorosuccinimide | HCID 31398 | — |
| Reactant | 1-Naphthalenecarboxaldehyde, oxime | HCID 240801 | — |
| Reactant | Methyl methylvinylphosphinate | HCID 6454580 | — |
| Product | Methyl 3-(1-naphthyl)-2-isoxazolin-5-yl(P-methyl)phosphinate | HCID 20062396 | 96.8% |
Reaction Steps
39.1 g (0.25 mol) of naphthaldoxime, 36.7 g (0.275 mol) of N-chlorosuccinimide, 33 g (0.275 mol) of methyl vinyl(P-methyl)phosphinate and 38.2 ml (0.275 mol) of triethylamine are reacted as in Example 1 to give 70 g of oily product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05006515 |
| Source dataset | uspto-grants-1991_04 |
| ORD ID | ord-f9619ce1e0f049b193c8db09d3cb2a25 |
| Source note | uspto-grants-1991_04 |