HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenylmaleic anhydride → Methyl 3-(2,5-dioxo-3-phenyl-2,5-dihydro-pyrrol-1-yl)-2-(2-methyl-[1,3]dioxolan-2-yl)propionate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenylmaleic anhydride | HCID 99174 | — |
| Reactant | Methyl 3-amino-2-(2-methyl-[1,3]dioxolan-2-yl)propionate | HCID 21982209 | — |
| Product | Methyl 3-(2,5-dioxo-3-phenyl-2,5-dihydro-pyrrol-1-yl)-2-(2-methyl-[1,3]dioxolan-2-yl)propionate | HCID 21982263 | — |
Reaction Steps
Methyl 3-(2,5-dioxo-3-phenyl-2,5-dihydro-pyrrol-1-yl)-2-(2-methyl-[1,3]dioxolan-2-yl)propionate was prepared (1.0 g, 56%) in the same manner as described in the above example 5 (1) from methyl 3-amino-2-(2-methyl-[1,3]dioxolan-2-yl)propionate (1.00 g, 5.29 mmol) and phenylmaleic anhydride (1.10 g, 6.34 mmol), and the obtained product was identified with the following NMR data.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07094908B2 |
| Source dataset | uspto-grants-2006_08 |
| ORD ID | ord-1f6ca9e302e948e0bf4ab1d4a60676d4 |
| Source note | uspto-grants-2006_08 |