Sulfuric Acid → HCID 13983555, compound

HRID 1084931Notes

Reaction equation

HRID 1084931 reaction equation
[OH:1][C:2]1[C:11]([CH2:12][CH:13]=[CH2:14])=[C:10]([Br:15])[CH:9]=[CH:8][C:3]=1[C:4]([O:6][CH3:7])=[O:5].[C:16](OC(=O)C)(=[O:18])[CH3:17].S(=O)(=O)(O)O>>[C:16]([O:1][C:2]1[C:11]([CH2:12][CH:13]=[CH2:14])=[C:10]([Br:15])[CH:9]=[CH:8][C:3]=1[C:4]([O:6][CH3:7])=[O:5])(=[O:18])[CH3:17]

Participants

4

Reactant 3

HCID 1118Sulfuric AcidHCID 7918Acetic AnhydrideHCID 13983554HCID 13983554, compound

Product 1

HCID 13983555HCID 13983555, compound

Procedure

254 g of methyl 2-hydroxy-3-allyl-4-bromobenzoate and 191 g of acetic anhydride were introduced into a 1-liter round-bottomed flask and 2 ml of sulphuric acid were then added.

Sources & evidence

ORD record
ord-dc715d6300a84a6595bb157d6a41fa0a
Source dataset
uspto-grants-1991_04
Patent number
US05006570

Reaction notes

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