Benzylamine → N-[5-(2-Phenylethoxy)pentyl]benzenemethanamine

HRID 1084956Notes

Reaction equation

HRID 1084956 reaction equation
Br[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][O:7][CH2:8][CH2:9][C:10]1[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=1.[CH2:16]([NH2:23])[C:17]1[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=1>>[C:10]1([CH2:9][CH2:8][O:7][CH2:6][CH2:5][CH2:4][CH2:3][CH2:2][NH:23][CH2:16][C:17]2[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=2)[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=1

Participants

3

Reactant 2

HCID 7504BenzylamineHCID 197980262-(5-Bromopentoxy)ethylbenzene

Product 1

HCID 20062790N-[5-(2-Phenylethoxy)pentyl]benzenemethanamine

Procedure

N-[5-(2-Phenylethoxy)pentyl]benzenemethanamine (8.6 g) was prepared in a similar manner from [2-[(5-bromopentyl)oxy]ethyl]benzene (10 g) and benzylamine (30 ml). The undistilled product was used without further purification in Example 1(c).

Workup

  1. distillationThe undistilled product was used without further purification in Example 1(c)

Sources & evidence

ORD record
ord-be51f40d356d420aa6a43fd1f47b8f49
Source dataset
uspto-grants-1991_04
Patent number
US05006556

Reaction notes

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