HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazine hydrate (1:1) → HCID 178482483, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazine hydrate (1:1) | HCID 24654 | — |
| Reactant | HCID 10444497 | HCID 10444497 | — |
| Catalyst | Nickel | HCID 935 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178482483 | HCID 178482483 | 106.5% |
Reaction Steps
3-(2-Methoxyethoxy)methyl-1-methyl-5-methylamino-4-nitropyrazole (0.73 g, 3 mmoles), hydrazine hydrate (0.5 ml) and Raney nickel (200 mg) were stirred in ethanol (12 ml) at 50° C. for 1.5 hours. The Raney Nickel was filtered off and the ethanol removed under reduced pressure yielding the title compound (0.64 g, 100%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05008263 |
| Source dataset | uspto-grants-1991_04 |
| ORD ID | ord-8cb38463871345fba65a18607599a7c0 |
| Source note | uspto-grants-1991_04 |