HCID 20061012, compound → HCID 20061030, compound

HRID 1085165Notes

Reaction equation

HRID 1085165 reaction equation
[CH3:1][NH:2][C:3]1[C:12]([N+:13]([O-])=O)=[CH:11][C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[N:4]=1.NC1C(COCCOC)=NNC=1NC>>[NH2:13][C:12]1[C:3]([NH:2][CH3:1])=[N:4][C:5]2[C:10]([CH:11]=1)=[CH:9][CH:8]=[CH:7][CH:6]=2

Participants

3

Reactant 2

HCID 20061012HCID 20061012, compoundHCID 178482483HCID 178482483, compound

Product 1

HCID 20061030HCID 20061030, compoundYield 97.3%

Procedure

2-Methylamino-3-nitroquinoline (711 mg, 3.5 mmol) was reduced according to the procedure of Preparation 11 (d) to give the title compound, (590 mg, 97%), m.p. 133°-136° C.

Sources & evidence

ORD record
ord-0504025b0ed544cfba774748d4039ac1
Source dataset
uspto-grants-1991_04
Patent number
US05008263

Reaction notes

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