HuagongsheHuagongshe Chemistry Print Report · For research reference only
tert-Butyl hydroperoxide → t-Amylperoxy 2,4-dimethylphenyl carbonate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | tert-Butyl hydroperoxide | HCID 6410 | — |
| Reactant | Phenyl chloroformate | HCID 15891 | — |
| Reactant | tert-Amyl hydroperoxide | HCID 76962 | — |
| Reactant | 2,4-Dimethylphenyl chloroformate | HCID 15917593 | — |
| Product | t-Amylperoxy 2,4-dimethylphenyl carbonate | HCID 54014625 | 65% |
Reaction Steps
A reaction was carried out in the same manner as described in Example 1, except that t-amyl hydroperoxide and 2,4-dimethylphenyl chloroformate were used in place of t-butyl hydroperoxide and phenyl chloroformate used in Example 1, to obtain 35.7 g (yield: 65%) of a compound having a GLC purity of 92%, which was a colorless liquid at room temperature.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05008353 |
| Source dataset | uspto-grants-1991_04 |
| ORD ID | ord-5d97dd5a689543be805316febca72878 |
| Source note | uspto-grants-1991_04 |