HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonium Acetate → HCID 14745923, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonium Acetate | HCID 517165 | — |
| Reactant | HCID 19902720 | HCID 19902720 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 14745923 | HCID 14745923 | 99.2% |
Reaction Steps
29.7 g (0.1 mol) of dibutyl dichloromaleate, 19.27 g (0.25 mol) of ammonium acetate and 40 ml of dimethylformamide were reacted under the same conditions as described in Example 1. 27.55 g (88.7% yield) of dibutyl aminochloromaleate were obtained as a reddish, viscous liquid (purity according to GC analysis 90%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05008392 |
| Source dataset | uspto-grants-1991_04 |
| ORD ID | ord-85b76cdd4c684433b474324969078d7b |
| Source note | uspto-grants-1991_04 |