HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,3-dimethyl-6-{2-[2-(4-nitrophenyl)ethylamino]-ethylamino}-2,4(1H,3H)-pyrimidinedione → 1,3-dimethyl-6-[2-(4-nitrobenzylamino)ethylamino]-2,4(1H,3H)-pyrimidinedione
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,3-dimethyl-6-{2-[2-(4-nitrophenyl)ethylamino]-ethylamino}-2,4(1H,3H)-pyrimidinedione | HCID 20061156 | — |
| Reactant | 1,3-dimethyl-6-[3-(4-nitroanilino)propylamino]-2,4-(1H,3H)-pyrimidinedione | HCID 20061244 | — |
| Product | 1,3-dimethyl-6-[2-(4-nitrobenzylamino)ethylamino]-2,4(1H,3H)-pyrimidinedione | HCID 20061366 | — |
Reaction Steps
The same procedure as in Example 2 was repeated with the exception that 1,3-dimethyl-6-(piperazin-1-yl)-2,4-(1H,3H)-pyrimidinedione (compound 2) was replaced with 0.45 g of 6-(2-aminoethylamino)-1,3-dimethyl-2,4(1H,3H)-pyrimidinedione (compound 13), in order to obtain 1,3-dimethyl-6-[2-(4-nitrobenzylamino)ethylamino]-2,4(1H,3H)-pyrimidinedione.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05008267 |
| Source dataset | uspto-grants-1991_04 |
| ORD ID | ord-e89c8c1262c146fbab5c36bb204f909f |
| Source note | uspto-grants-1991_04 |