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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1085265Generated: October 26, 2026

p-Fluoronitrobenzene → N,N', N"-trimethyl-N-(4-nitrophenyl)diethylenetriamine

https://huagongshe.com/reaction/1085265

Reaction equation

Participants

RoleNameHCIDCharge
Reactantp-FluoronitrobenzeneHCID 9590—
Reactant1,4,7-TrimethyldiethylenetriamineHCID 66930—
SolventDimethyl SulfoxideHCID 679—
ProductN,N', N"-trimethyl-N-(4-nitrophenyl)diethylenetriamineHCID 21625360—

Reaction Conditions

Temperature120 °C

Reaction Steps

In 7 ml of dimethyl sulfoxide were dissolved 1.41 g of p-fluoronitrobenzene and 14 g of N,N',N"-trimethyldiethylenetriamine, and the mixture was then stirred at 120° C. for 3 hours.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05008267
Source datasetuspto-grants-1991_04
ORD IDord-ea800a3811824a62a5c3612ba298168a
Source noteuspto-grants-1991_04